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Determination of carbendazim residues in fruits vegetables and cereals by HPLC with column switching

100%

Michel M., Buszewski B.

Journal of Plant Protection Research

2002

tom 42

nr 1

Method for determination of carbendazim residues in fruits, vegetables and cereals was described. The compound was extracted with methanol-hydrochloric acid mixture, and after liquid-liquid partition step with dichloromethane, was determined by high performance liquid chromatography (HPLC) with column switching and ultraviolet (UV) detection. The average recoveries of carbendazim from fortified sample were from 68.7% ± 4.3% to 92.6% ± 4.5%, the coefficients of variation were from 2.9% to 6.3%, and the limits of quantification at λ = 279 nm were from 0.02 mg/kg to 0.2 mg/kg.

Ograniczanie wyników

1 Journal of Plant Protection Research

1 Buszewski B.

1 Michel M.

1 2002

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Determination of carbendazim residues in fruits vegetables and cereals by HPLC with column switching