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Determination of metoprolol and its metabolites in human urine by capillary isotachophoresis

100%

Sadecka J., Polonsky J., Shintani H.

Polish Journal of Environmental Studies

1997

tom 06

nr 2

The separation and determination of metoprolol and its metabolites M I (metoprolol acid), M II (2-hydroxy-3-(4-metoxyethylphenoxy)-propanoic acid, M III (a-hydroxymetoprolol) and H 105 (O-desmethylmetoprolol) in human urine by capillary isotachophoresis were investigated. Metoprolol and metabolites M I, M III and H 105 were separated by cationic isotachophoresis in the electrolyte system sodium acetate buffer (pH 5.0) (c,=10 mM) -ß-alanine. Metabolite M II was separated using the anionic electrolyte system histidine hydrochloride buffer (pH 6.0) (cL = 10 mM) -morpholinoethane-sulfonic acid. Endogenous and the possible exogenous compounds were almost totally removed from urine by solid-phase extraction using a SepPak Cls cartridge. The recovery of compounds varied from 84.6 to 95.8%. The linear calibration range was studied for eventual application of the method to real urine samples. Limit of determination was 0.5 mg/ml.

Beta-adrenergic antagonists influence abdominal aorta contractility by mechanisms not involving beta-adrenergic receptors

84%

Hauzer W., Bujok J., Czerski A., Rusiecka A., Pecka E., Gnus J., Zawadzki W., Witkiewicz W.

Folia Biologica

2014

tom 62

nr 3

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Influence of an early adrenergic blockade on thrombotic infarct size and myocardial metabolism

67%

Zmudka K., Dubiel J., Pieniazek P., Dudek D., Kocurek A., Trebacz J., Grodecki J., Flameng W., De Geest H.

Journal of Physiology and Pharmacology

1998

tom 49

nr 3

Zastosowanie leków przeciwarytmicznych klasy II wg Vaughana Williamsa u psów i kotów

59%

Noszczyk-Nowak A., Michalek M., Cepiel A., Szczypka M.

Weterynaria w Praktyce

2015

tom 12

nr 10

Ograniczanie wyników

1 Folia Biologica

1 Journal of Physiology and Pharmacology

1 Polish Journal of Environmental Studies

1 Weterynaria w Praktyce

1 Bujok J.

1 Cepiel A.

1 Czerski A.

1 De Geest H.

1 Dubiel J.

1 Dudek D.

1 Flameng W.

1 Gnus J.

1 Grodecki J.

1 Hauzer W.

1 Kocurek A.

1 Michalek M.

1 Noszczyk-Nowak A.

1 Pecka E.

1 Pieniazek P.

1 Polonsky J.

1 Rusiecka A.

1 Sadecka J.

1 Shintani H.

1 Szczypka M.

1 Trebacz J.

1 Witkiewicz W.

1 Zawadzki W.

1 Zmudka K.

1 2015

1 2014

1 1998

1 1997

Wyniki wyszukiwania

Determination of metoprolol and its metabolites in human urine by capillary isotachophoresis

Beta-adrenergic antagonists influence abdominal aorta contractility by mechanisms not involving beta-adrenergic receptors

Influence of an early adrenergic blockade on thrombotic infarct size and myocardial metabolism

Zastosowanie leków przeciwarytmicznych klasy II wg Vaughana Williamsa u psów i kotów