Usefulness of GC-MS method for the determination of DDT, DMDT, and y-HCH in bees (bodies) for legal purposes

• Autorzy: Banka K. , Buszewicz G. , Listos P. , Madro R.
• Języki publikacji: EN

Abstrakty

EN

The paper contains the description of mass poisoning of honey bees and the method used to determine dichlorodiphenyltrichloroethane, methoxychlor, and lindane in the insects. The ultrasound-aided extraction of pesticides from dead bees was conducted using dichloromethane and the analysis of the extracts was conducted using gas chromatography-mass spectrometry. The whole procedure was vatidated.

Słowa kluczowe

EN

honey bee; bee; poisoning; organochlorine insecticide; insecticide; analytical method

• Wydawca: -
• Czasopismo: Bulletin of the Veterinary Institute in Puławy
• Rocznik: 2010
• Tom: 54
• Numer: 4
• Opis fizyczny: p.655-659,fig.,ref.

Twórcy

autor

Banka K.

• Chair and Department of Forensic Medicine, Medical University, 20-090 Lublin, Poland

autor

Buszewicz G.

autor

Listos P.

autor

Madro R.

Bibliografia

• 1. Backlund P., Holmbom B., Leppäkoski E.: Industrial Emissions and Toxic Pollutants. The Baltic University Secretariat, Uppsala University, Pppsala, Sweden, 1993.
• 2. Bhatnagar V.K., Patel J.S., Variya M.R., Venkaiah K., Shah M.P., Kashyap S.K.: Levels of organochlorine insecticides in human blood from Ahmedabad (rural), India. Bull Environ Contaminat Toxicol 1992, 48, 302- 307.
• 3. Blasco C., Lino C.M., Picó Y., Pena A., Font G., Silveira M.I.: Determination of organochlorine pesticide residues in honey from the central zone of Portugal and the Valencian community of Spain. J Chromatogr A 2004, 1049, 155-160.
• 4. Brzeziński J., Szutowski M.M.: Toxicology of pesticides. In: Modern toxicology. Editor Seńczuk W., PZWL, Warszawa, 2006.
• 5. Chen F., Chen L., Wang Q., Zhou J., Xue X., Zhao J.: Determination of organochlorine pesticides in propolis by gas chromatography-electron capture detection using double column series solid-phase extraction. Anal Bioanal Chem 2009, 393, 1073-1079.
• 6. Czaplicki E., Podgórska B., Rogalińska M., Stobiecki S.: Environmental fate of POPs in agricultural location (experience of Poland). Proceedings of the Subregional Awareness Raising Workshop on Persistent Organic Pollutants (POPs), Kranjska Gora, Slovenia, 1998.
• 7. EXTOXNET, Extension Toxicology Network. A pesticide information project of cooperative extension offices. USDA/Extension Service/National Agricultural Pesticide Impact Assessment Program, 1996, (http://extoxnet.orst. edu/pips/methoxyc.htm).
• 8. EXTOXNET, Extension Toxicology Network. A pesticide information project of cooperative extension offices. USDA/Extension Service/National Agricultural Pesticide Impact Assessment Program, 1996, (http://extoxnet.orst. edu/pips/ddt.htm).
• 9. Fernández Muíño M.A., Simal Lozano J.: Simplified method for the determination of organochlorine pesticides in honey. Analyst 1991, 116, 269-271.
• 10. Frenich A.G., Bolaños P.P., Vidal J.L.: Multiresidue analysis of pesticides in animal liver by gas chromatography using triple quadrupole tandem mass spectrometry. J Chromatogr A 2007, 1153, 194-202.
• 11. Hoffmann E., Charette J., Stroobant V.: Mass spectrometry. Ed. Wydawnictwo Naukowo-Techniczne, Warszawa, 1994.
• 12. Jiménez J.J., Bernal J.L., del Nozal M.J., Alonso C.: Liquid-liquid extraction followed by solid-phase extraction for the determination of lipophilic pesticides in beeswax by gas chromatography-electron-capture detection and matrix-matched calibration. J Chromatogr A 2004, 1048, 89-97.
• 13. Kolankaya D., Erkmen B., Sorkun K., Koçak O.: Pesticide residues in honeybees and some honeybee products in Turkey. Pesticidi 2002, 17, 73-84.
• 14. National Implementation Plan for the Stockholm Convention, Warszawa, 2004, http://pdc.ceu.hu/ archive/00002817/01 /NIP-Poland-eng.pdf
• 15. Niewiadowska A., Semeniuk S., Żmudzki J.: Pesticide residues in food of animal origin in 1997-2006 in Poland. Medycyna Wet 2008, 64, 1221-1224.
• 16. PAN International List of Highly Hazardous Pesticides, 1/2009 (http://www.pan-germany.org/ download/PAN_HHP-List_090116.pdf).
• 17. Piotrowski J.: Basics of toxicology. Ed. WNT, Warszawa, 2006.
• 18. Przybyłowski P., Wilczyńska A., Rój A.: Organochlorine pesticide residues in honeys. Bromat Chem Toksykol 2003, suppl, 333-337.
• 19. Rissato S.R., Galhiane M.S., de Almeida M.V., Gerenutti M., Apon B.M.: Multiresidue determination of pesticides in honey samples by gas chromatography- mass spectrometry and application in environmental contamination. Food Chem 2007, 101, 1719-1726.
• 20. Sasaki K., Ishizaka T., Suzuki T., Takeda M., Uchiyama M.: Accumulation levels of organochlorine pesticides in human adipose tissue and blood. Bull Environ Contamin Toxicol 1991, 46, 662-669.
• 21. Schapira A.: DDT: a polluted debate in malaria control. Lancet 2006, 368, 2111-2113.
• 22. Spodniewska A., Romaniuk K.: Chlorinated hydrocarbons in bees from a select apiary of Piska Forest in 1996-2005. Medycyna Wet 2007, 63, 247-249.
• 23. Spodniewska A., Romaniuk K.: Residues of chlorinated hydrocarbons in bees in relation to apiary location. Medycyna Wet 2006, 62, 1200-1201.
• 24. Struciński P., Górlaczyk K., Ludwicki J.K., Czaja K., Hernik A., Korcz W.: Levels of selected organochlorine insecticides, polychlorinated biphenyls, phthalates and perfluorinated aliphatic substances in blood - Polish WWF study. Roczn PZH 2006, 57, 99-112.
• 25. Tsipi D., Triantafyllou M., Hiskia A.: Determination of organochlorine pesticide residues in honey, applying solid phase extraction with RP-C18 material. Analyst 1999, 124, 473-475.
• 26. Wilczynska A., Przybylowski P.: Residues of organochlorine pesticides in Polish honeys. APIACTA 2007, 42, 16-24.
• 27. World Health Organization (WHO). Environmental health Criteria 83, DDT and its derivatives environmental effects. World Health Organization, Geneva, Switzerland, 1989.
• 28. Tahboub Y.R., Zaater M.F., Barri T.A.: Simultaneous identification and quantitation of selected organochlorine pesticide residues in honey by full-scan gas chromatography-mass spectrometry. Analyt Chim Acta 2006, 558, 62-68.