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2010 | 50 | 3 |

Tytuł artykułu

Oznaczanie pozostałości herbicydów z grupy fenoksykwasów w wodzie, glebie, ziarnie i słomie zbóż techniką chromatografii cieczowej

Warianty tytułu

EN
Determination of phenoxyacid herbicides in water, soil, grain and straw by liquid chromatography

Języki publikacji

PL

Abstrakty

EN
Phenoxyacetic acid herbicides is a group very similar in chemical structure to compounds widely used in plant protection products applicable to weed control in cereals, grass seed, corn, and also used for late treatment in cereals. This paper describes a liquid chromatographic method for determining phenoxyacetic acid herbicides in plant material, soil and water. The method for determining residues of phenoxyacetic acid herbicides allows their determination at low concentrations while retaining excellent statistical parameters.

Wydawca

-

Rocznik

Tom

50

Numer

3

Opis fizyczny

s.1452-1458,tab.,bibliogr.

Twórcy

autor
  • Terenowa Stacja Doświadczalna, Instytut Ochrony Roślin – Państwowy Instytut Badawczy, ul.Chełmońskiego 22, 15-195 Białystok
autor
autor
autor

Bibliografia

  • Baggiani C., Giovannoli C., Anfossi L., Tozzi C. 2001. Molecularly imprinted solid-phase extraction sorbent for the clean-up of chlorinated phenoxyacids from aqueous samples. J. Chromatogr. A 938: 35–44.
  • Catalina M.I., Dallüge J., Vreuls R.J.J., Brinkman U.A.T. 2000. Determination of chlorophenoxy acid herbicides in water by in situ esterification followed by in-vial liquid-liquid extraction combined with large-volume on-column injection and gas chromatography-mass spectrometry. J. Chromatogr. A 877: 153–166.
  • Diez C., Traag W.A., Zommer P., Marinero P., Atienza J. 2006. Comparison of an acetonitrile extraction/partitioning and „dispersive solid-phase extraction” method with classical multiresidue methods for the extraction of herbicide residues in barley samples. J. Chromatogr. A 1131: 11–23.
  • Document N° SANCO/10684 2009. Metod Validation and Quality Control Procedures for Pesticide Residues Analysis in Food and Feed.
  • Farran A., Ruiz S. 2004. Application of solid-phase extraction and micellar electrokinetic capillary chromatography to the study of hydrolytic and photolytic degradation of phenoxy acid and phenylurea herbicides. J. Chromatogr. A 1024: 267–274.
  • Garcia-Reyes J.F., Hernando M.D., Ferrer C., Molina-Diaz A., Fernández-Alba A.R. 2007. Large Scale Pesticide Multiresidue Methods in Food Combining Liquid Chromatography – Time-of-Flight Mass Spectrometry and Tandem Mass Spectrometry. Anal. Chem. 79: 7308–7323.
  • Luque-Garcia J.L., Luque de Castro M.D. 2002. Coupling continuous subcritical water extraction, filtration, preconcentration, chromatographic separation and UV detection for the determination of chlorophenoxy acid herbicides in soils. J. Chromatogr. A 959: 25–35.
  • Praczyk T., Skrzypczak G. 2004. Herbicydy. PWRiL, Poznań, 274 ss.
  • Polska Norma – PN-R-04113: 1997. Materiał roślinny i gleba. Oznaczanie pozostałości herbicydów. Substancja aktywna – pochodne fenoksykwasów. Wyd. Norm., Warszawa.
  • Quintana J.B., Rodil R., Muniategui-Lorenzo S., Lopez-Mahia P., Parada-Rodriguez D. 2007. Multiresidue analysis of acidic and polar organic contaminants in water samples by stir-bar sorptive extraction-liquid desorption – gas chromatography-mass spectrometry. J. Chromatogr. A 1174: 27–39.
  • Rodriguez I., Rubi E., Gonzalez R., Quintana J.B., Cela R. 2005. On-fibre silylation following solid-phase microextraction for the determination of acidic herbicides in water samples by gas chromatography. Anal. Chim. Acta 537: 259–266.
  • Santos-Delgado M.J., Crespo-Corral E., Polo-Diez L.M. 2000. Determination of herbicides in soil samples by gas chromatography: optimization by the simplex method. Talanta 53: 367–377.
  • Wu J., Ee K.H., Lee H.K. 2005. Automated dynamic liquid–liquid–liquid microextraction followed by high-performance liquid chromatography-ultraviolet detection for the determination of phenoxy acid herbicides in environmental waters. J. Chromatogr. A 1082: 121–127.
  • Yu L.Z., Wells M.J.M. 2007. Establishing the feasibility of coupled solid-phase extraction-solidphase derivatization for acidic herbicides. J. Chromatogr. A 1143: 16–25.

Typ dokumentu

Bibliografia

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Identyfikator YADDA

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