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2008 | 52 | 3 |

Tytuł artykułu

Analytical procedure for the determination of fluoroquinolones in animal muscle

Warianty tytułu

Języki publikacji

EN

Abstrakty

EN
A liquid chromatography-fluorescence detection method for the determination of five fluoroquinolones in muscle tissue was proposed. The method is selective and robust enough for the required purposes. The whole procedure was validated in accordance with the Commission Decision 657/2002/EC. Detection capabilities were from 132.8 to 421.0 µg/kg, and recoveries ranged from 51.7% to 80.91%, depending on the analyte.

Wydawca

-

Rocznik

Tom

52

Numer

3

Opis fizyczny

p.427-430,fig.,ref.

Twórcy

autor
  • National Veterinary Research Institute, 24-100 Pulawy, Poland
autor

Bibliografia

  • 1. Anon.: Commission Decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. O J 2002, L 221, 8-36.
  • 2. Anon.: Council Directive 96/23/EC of 29 April 1996 on measures to monitor certain substances and residues thereof in live animals and animal products and repealing Directives 85/358/EEC, 86/469/EEC and Decision 89/187/EEC and 91/664/EEC. O J 1996, L 125, 10-31.
  • 3. Anon.: ISO/11843: Capability of detection (Part 1): Terms and definitions (Part 2): Methodology in the linear calibration case. International Organization for Standardization, 2000.
  • 4. Bailac S., Ballesteros O., Jimenez-Lozano E., Barron D., Sanz-Nebot V., Navalon A., Vilchez J.L., Barbosa J.: Determination of quinolones in chicken tissues by liquid chromatography with ultraviolet absorbance detection. J Chromatogr A 2004, 1029, 145-151.
  • 5. Brown S.A.: Fluoroquinolones in animal health. J Vet Pharmacol Ther 1996, 19, 1-14.
  • 6. Council Regulation 2377/90EC. Off J Eur Commun, 1990, L224.
  • 7. Hernandez-Arteseros J.A., Barbosa J.M., Compario R., Prat M.D.: Analysis of quinolone residues in edible animal products. J Chromatogr A 2002, 945, 1-24.
  • 8. Martinez M., Mcdermott P., Walker R.: Pharmacology of the fluoroquinolones: a perspective for the use in domestic animals. Vet J 2006, 173, 10-28.
  • 9. Posyniak A., Zmudzki J., Semeniuk S., Niedzielska J., Eblis R.: Determination of fluoroquinolone residues in animal tissues by liquid chromatography. Biomed Chromatogr 1990, 13, 279-285.
  • 10. Posyniak A., Zmudzki J., Mitrowska K.: Dispersive solid-phase extraction for the determination of sulfonamides in chicken muscle by liquid chromatography. J Chromatogr A 2005, 1087, 259-264.
  • 11. Ramos M., Aranda A., Garcia E., Reuvers T., Hooghuis H.: Simple and sensitive determination of five quinolones in food by liquid chromatography with fluorescence detection. J Chromatogr B 2003, 789, 373- 381.
  • 12. Toussaint B., Chedin M., Bordin G., Rodriguez A.R.: Determination of (fluoro)quinolone antibiotic residues in pig kidney using liquid chromatography-tandem mass spectrometry. J Chromatogr A 2005, 1088, 32-39.
  • 13. Van Hoof N., De Wasch K., Okerman L., Reybroeck W., Poelmans S., Noppe H., De Brabander H.: Validation of a liquid chromatography-tandem mass spectrometric method for the quantitation of eight quinolones in bovine muscle, milk and aquacultured products. Anal Chim Acta 2005, 529, 265-272.
  • 14. Verdon E., Coudedor P., Roudault B., Sanders P.: Multiresidue method for simultaneous determination of ten quinolone antibacterial residues in multimatrix/multispecies animal tissues by liquid chromatography with fluorescence detection: single laboratory validation study. J AOAC Int 2005, 88, 1179- 1192.
  • 15. Yorke J.C., Froc P.: Quantitation of nine quinolones in chicken tissues by high-performance liquid chromatography with fluorescence detection. J Chromatogr A 2000, 882, 63-77.

Typ dokumentu

Bibliografia

Identyfikatory

Identyfikator YADDA

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