Possibilities and limitations of supercritical fluid extraction [SFE] as a sample preparation technique

• Autorzy: Kot A. , Sandra P. , Kolodziejczyk A.M.
• Języki publikacji: EN

Abstrakty

EN

This review focuses on different attempts to understand the process during extraction • sing supercritical fluids and on different approaches to obtain quantitative and selective extractions. Supercritical fluid extraction is a fast technique and, unlike other methods of extraction, allows several sample preparation steps to be incorporated within the extraction step. The authors consider the possible methods of optimisation of the SFE variables - fluid type, modifiers of the fluid, pressure (density), temperature, flow rate, sample size, analyte collection, and fixation - to help an analyst to extract the solutes of interest in a quantitative way while avoiding or minimising co-extraction of other matrix components.

Słowa kluczowe

EN

priority pollutant; sample preparation; selectivity; supercritical fluid extraction

• Wydawca: -
• Czasopismo: Polish Journal of Environmental Studies
• Rocznik: 1996
• Tom: 05
• Numer: 6
• Opis fizyczny: p.5-15,fig.,ref.

Twórcy

autor

Kot A.

• Technical University of Gdansk, Narutowicza Str.11-12, 80-952 Gdansk, Poland

autor

Sandra P.

autor

Kolodziejczyk A.M.

Bibliografia

• ZOSEL K. Angew. Chem. 90, 748, 1978.
• SAITO M., YAMAUCHI Y. Supercritical Fluid Extraction and Supercritical Fluid Chromatography for Preparative Separation, JASCO Report Publisher, Tokyo, Japan, 1990.
• ANDERSEN M. R., SWANSON J. T., PORTER N. L., RICHTER B. E. J. Chromatogr. Sci. 27, 371-377, 1989.
• LEE M. L., MARKIDES K. E. Analytical Supercritical Fluid Chromatography and Extraction, Chromatography Conferences, Inc. Provo, Utah, 313-362, 1990.
• POOLE C. F., POOLE S. K. Chromatography Today, Elsevier Science Publishers B. V. 1991.
• KING J. W. J. Chromatogr. Sci. 27, 355-363, 1989.
• RICHARDS M., CAMPBELL R. M., LC GC Intl. 7(4), 33-36, 1991.
• GERE D., DERRICO E. M., LC GC Intl. 7(6), 325-331, 1994.
• GERE D., DERRICO E. M., LC GC Intl. 7(7), 370-375, 1994.
• PIPKIN W., LC GC Intl. 5(1), 8-10, 1992.
• KOT A., PhD Thesis, 1995.
• NAMIEŚNIK J., ZYGMUNT B., BIZIUK M., WIERGOWSKI M., TORRES L. Pol. J. Environ. Stud., 5(1), 5-26, 1996.
• RIEKKOLA M. L., MANNINEN P., HARTONEN. Hyphenated techniques in supercritical fluid Chromatography and extraction, ed K. Jinno, Elsevier Sci. Publ. 275-304, 1992.
• DAVIES I. L., RAYNOR M. W., KITHINJI ] . P., BARTLE K. D., WILLIAMS P. T., ANDREWS G. E., Anal. Chem. 60, 683A-702A. 1988.
• ENGELHARDT W. G., GARGUS A. G. Am. Lab. 20(2), 30-32, 1988.
• LOHLEIT M., BACHMANN K. J. Chromatogr. 505, 227, 1990.
• WANG X. Y., BARTHA R., ROSEN J. D. Environ. Sci., Tech-noi. 24, 1732, 1990.
• LEVY J. M., ROSSELLI A. C., STOROZYNSKY E., RAVEY R. DOLAT A L. A., ASHRAF-KHORASSANI M., LC GC, 106), 396, 1992.
• SNYDER J. L. GROB R. L., NALLY M. E., OOSTDYK T. S. J. Chromatogr. Sci. 31(5), 183, 1993.
• SANDRA P., KOT A., CASTANHO J., DAVID F. Int. Environ. Technol, 4(5), 10, 1994.
• SANDRA P., KOT A., DAVID F. Chemistry Today, 12(9), 33-39, 1994.
• SANDRA P., KOT A., MEDVEDOVICI A., DAVID F. J. Chromatogr. A, 703, 467, 1995.
• SANDRA P., KOT A., DAVID F. Proc. 16th International Symposium on Capillary Chromatography, Riva del Garda, Italy - 24-27.05.1993, Eds. Sandra P., Markides K., Publ. Huthig Verlag, Heidelberg, Germany, pp. 1515-1519, 1994.
• BOWADT S., JOHANSSON B. Anal. Chem., 66, 667-673, 1994.
• SNYDER J. L., GROB R. L., MC NALLY M. E., DOSTDYK T. S. Anal. Chem. 64(17), 1940-1946, 1992.
• ONUSKA F. I., TERRY K. D., WILKINSON R. J., J. High Resolut. Chromatogr. 16, 407-412, 1993.
• RICHARDS M., CAMPBELL R. M., LC GC Intl. 4(7), 33-36, 1991.
• BURFORD M. D., HAWTHORNE S. B., MILLER D. J. Anal. Chem. 64, 1497-1505, 1993.
• SCHANTZ, CHESLER S. N. J. Chromatogr. 363, 397-401, 1986.
• VAN der WELDE, de HAAN E. G., LIEM A. K. D. J. Chromatogr. 626, 135-143, 1992.
• DAVID F., KOT A., VANLUCHENE E., SIPPOLA E., SANDRA P. Proc. 15th International Symposium on Capillary Chromatography, Riva del Garda, Italy - 24-27.05.1993, Eds. Sandra P., Markides K., Publ. Huthig Verlag, Heidelberg, Germany, pp. 1572-1577, 1993.
• LANGENFELD J. L., HAWTHORNE S. B., MILLER D. J., PAWLISZYN J. Anal. Chem. 65, 338-344, 1993.
• ALEXANDROU N., PAWLISZYN J. Anal. Chem. 61, 2770, 1989.
• HAWTHORNE S. B., MILLER D. J., LANGENFELD J. J. J. Chromatogr. Sci. 28, 2, 1990.
• HAWTHORNE S. B., MILLER D. J. Anal. Chem. 59, 1705-1708, 1987.
• HAWTHORNE S. B., LANGENFELD J. J., MILLER D. J., BURFORD M. D. Anal. Chem. 64, 1614-1622, 1992.
• HAWTHORNE S. B., YANG Y., MILLER D. J. Anal. Chem. 66, 2912-2920, 1994.
• GIDDINGS J. C., MYERS M. N., LAREN L. MC, KELLER R. A. Science, 162, 67-69, 1968.
• PAGE S. H., GOATES S. R., LEE M. L. ]. Super Fluid, 4, 109-117, 1991.
• FAHMY T. M., PAULAITIS M. E., JOHNSON D. M., MC NALLY M. E. P. Anal. Chem. 65, 1462-1469, 1993.
• HOWARD J. L., TAYLOR L. T. ]. High Res. Chrom. 16, 39-45, 1993.
• CROSS R. F., EZZELL J. L., PORTER N. L., RICHTER B. E. Int. Lab. 24(11), 23-28, 1994.
• SCHWEIGHARDT F. K., MATHIAS P. M. J. Chromatogr. Sci. 31, 207-211, 1993.
• VIA J., TAYLOR L. T., SCHWEIGHARDT F. K. Anal. Chem. 66, 1459, 1994.
• WUCHNER K., GHIJSEN R. T., BRFINKMAN R., GROB R., MATHIEU J. Analyst, 118, 11, 1993.
• DAVID F., VERSCHUERE M., SANDRA P. Fresenius J. Anal. Chem. 344, 479-485, 1992.
• LANGELFELD J. J., HAWTHORNE S. B., MILLER D. J., PAWLISZYN J. Anal. Chem. 66, 909, 1994.
• DANKERS J., GROENENBOOM M., SCHOLTIS L. H. A., VAN DER HEIDEN C. J. Chromatogr. 641, 357, 1993.
• WHEELER J. R., MC NALLY M. E. J. Chromatogr. Sci. 27, 534, 1989.
• LEE H., PEART T. E., HONG-YOU R. L., GERE D. R. J. Chromatogr. A, 653, 83, 1993.
• BOWADT S., HAWTHORNE S. B. J. Chromatogr. 703, 549-571, 1995.
• DEYE J. F., BERGER T. A. Anal. Chem. 62, 615, 1990.
• DAVID F., KOT A., VANLUCHENE E., SIPPOLA E., SANDRA P. Proc. The Second European Symposium on Analytical SFC and SFE, Riva del Garda, Italy, Eds. Sandra P., Markides K., Publ. Huthig Verlag, Heidelberg, Germany, pp. 10-16, 1993.
• BURFORD M. D., HAWTHORNE S. B., MILLER D. J. Anal. Chem. 64, 1497-1505, 1993.
• REINDL S., HOFLER F. Anal. Chem. 66, 1808-1816, 1994.
• PAWLISZYN J. private communication.
• MUNDER A., CHRISRENSEN R. G., WISE S. A. J. Microcol. Sep. 3, 127-140, 1991.
• PAWLISZYN J. J. Chromatogr. Sci. 31, 31, 1993.
• HAWTHORNE S. B., MILLER D. J. Chromatogr. 403, 63-76, 1987.
• KING J. W., JOHNSON J. H., FRIEDRICH J. P. Agric. Food Chem. 37, 951, 1989.
• HAWTHORNE S. B. Anal. Chem 62(11), 633A-642A, 1990.
• BOWADT S., HAWTHORNE S. B. J. Chromatogr. A, 703, 549-571, 1995.
• LOPEZ-AVILA V., DODHIWALA N. S., BECKERT W. F. J. Chromatogr. Sci. 28, 468, 1990.
• BUFORD M. D., HAWTHORNE S. B., MILLER D. J., BRAGGINS T. J. Chromatogr. 609, 321, 1992.
• LANGELFELD J. J., BURFORD M. D., HAWTHORNE S. B., MILLER D. J. J. Chromatogr. 594, 297, 1992.
• MEYER A., KLEIBOHMER J. Chromatogr. A, 657, 327, 1993.
• KOT A., DAVID F., SANDRA P. Proc. of the V Polish Conference on Analytical Chemistry, Gdańsk 03.09-08.09.1995. Kom. Chem. Anal. PAN - Poland, t. 2 pp. 389-390, 1995.
• BOWADT S., JOHANSSON B., PELUSIO F., LARSEN B. R., ROVIDA C. ]. Chromatogr. 662, 424, 1994.
• MULCAHEY L. J., HEDRICK J. L., TAYLOR L. T. Anal. Chem. 63, 2225-2232, 1991.
• SANDRA P., KOT A., TRANG K., DAVID F. The European Food and Drink Review, Summer, pp- 69-75, 1994.
• SUGIYAMA K., SAITO M., HONDO T., SENDA M. J. Chromatogr. 332, 107-116, 1985.
• MC NALLY M. E. P.,-WHEELER J. R. ] . Chromatogr. 435, 63-71, 1988.
• MIAO Z., YANG M. J., PAWLISZYN J. J. Chromatogr. Sci. 33(9), 493-499, 1995.
• LEVY J. M., CAVALIER R. A., BOSCH T. N., RYNASKI A. M., HUHAK W. E. J. Chromatogr. Sci., 27, 341, 1989.
• HAWTHORNE 8. B., MILLEER D. J., KRIEGER M. S. J. Chromatogr. Sci., 27, 347, 1989.
• WRIGHT B. W., FRYE S. R., MC MINN D. G., SMITH R. D. Anal. Chem. 59, 640, 1987.
• GRAZFELD-HUSGEN A., SCHUSTER R., SCHULENBERG-SCHELL H. Int. Lab. June, 15-21, 1994.
• ASHRAF-Kl-IORASSANI M., GIDANIAN S., YAMANI Y. J. Chromatogr. Sci. 33(11), 658-662, 1995.
• BAIN F., HAERDI W. Proc. Second European Symposium on Analytical SFC and SFE, Riva del Garda, Italy, 1993, Eds. Sandra P. and Markides K., Huethig, Heidelberg, Germany, pp. 209-210, 1993.
• CAMEL V., CAUDE M., TAMBUTE A. J. Chromatogr. Sci. 33, 123-132, 1995.
• FAHMY T. M., PAULAITIS M. E., JOHNSON D. M., MC NALLY M. E. P. Anal. Chem. 65, 1462-1469, 1993.
• ONUSKA F. I., TERRY K. A. J. High Resolut. Chromatogr. 12, 357-361, 1989.
• MC NALLY M. E. P., WHEELER J. R. J. Chromatogr. 447, 53-63, 1988.
• ASHRAF-KHOTASSANI M., TAYLOR L. T. Anal. Chem. 61, 145, 1989.
• CORTES H. J., GREEN L. S., CAMPBELL R. M. Ana]. Chem. 63, 2719-2724, 1991.
• BOWADT F., PELUSIO F., MONTANARELLA L., LARSEN B., MAPELLI G. Proc. Second European Symposium on Analytical SFC and SFE, Riva del Garda, Italy, 1993, Eds. Sandra P. and Markides K., Huethig, Heidelberg, Germany, pp. 114-120, 1993.
• JANDA V., STEENBEKE, SANDRA P. J. Chromatogr. 479, 200-205, 1989.
• HO J. S., TANG P. H., EICHELBERGER J. W., BUDDE W. L. J. Chromatogr. Sci. 33(1), 1-8, 1995.
• MC EACHERN P. R., FOSTER G. D. J. Chromatogr. 632, 119-125, 1993.
• MESSER D. C., TAYLOR L. T. J. Chromatogr. Sci. 33(1), 290-296, 1995.
• HOWARD A. L., TAYLOR L. T. J. Cheomatogr. Sci. 30, 374-382, 1992.
• SANDRA P., KOT A., DAVID F. Proc. of the International Symposium on Chromatography, H. Hatano and T. Hanai (Eds), Publ. World Sientific, Singapore, p. 1805-1809, 1995.
• SANDRA P., MEDVEDOVICI A., KOT A., DAVID F. Int. Environ. Technol., 5(3), 10, 1995.
• SANDRA P., KOT A. Proc. of the V Polish Conference on Analytical Chemistry, Gdańsk 03.09-08.09.1995. Kom. Chem. Anal. PAN - Poland, t. 1 pp. 28-30, 1995.
• KOT A., DAVID F., SANDRA P. Proc. 16th International Symposium on Capillary Chromatography, Riva del Garda, Italy - 26-30.09.l994, Eds. Sandra P. and Markides K., Huethig, Heidelberg, Germany, pp. 1637-1648, 1994.
• BAYONA J. M., CAI Y. J. Chromatogr. Sci. 33(3), 89-97, 1995.
• SANDRA P., KOT A., DAVID F. Proc. of the International Symposium on Solid Phase Extraction, Publ. Advanstar, UK 1994, p. 183-189, 1994.
• THIEBAULT D., CHERVET J.-P., VANNOORT R. W., JONG G. J., BRINKMAN U. A. Th., FREI R. W. J. Chromatogr. 477, 151, 1989.
• RAMSEY E. D., PERKINS J. R., GAMES D. E., STARTIN J. R. J. Chromatogr. 464, 353, 1989.
• .XIE Q. L., MARKIDES K. E., LEE M. L. J. Chromatogr. Sci. 27, 365, 1989.
• SAITO M., YAMAUCHI Y., INOMATA K., KO'ITKAMP W. P. ]. Chromatogr. Sci. 27, 79, 1989.
• ENGELHARDT H., GFOSS A. J. High Resolut. Chromatogr. Chromatogr. Commun. 11, 38, 1988.
• BERG B. E., HANSEN E. M., GREIBROKK T. Proc. Second European Symposium on Analytical SFC and SFE, Riva del Garda, Italy, Eds. Sandra P. and Markides K., Huethig, Heidelberg, Germany, pp. 194-202, 1993.
• HAWTHORNE S. B., KRIEGER M. S., MILLER D. J. Anal. Chem. 60, 472, 1988.
• AHMAD M., BERRY A. J., RAMSEY E. D. Proc. Second European Symposium on Analytical SFC and SFE, Riva del Garda, Italy, Eds. Sandra P. and Markides K., Huethig, Heidelberg, Germany, pp. 282-283, 1993.
• SCHNEIDERMAN M. A., SHARMA A. K., MAHANAMA K. R. R., LOCKE D. C. J. Assoc. Off. Anal. Chem., 71, 815, 1988.
• FRONING G. W., WEHLING R. L., CUPPETT S. L., PIERCE M. M., NIEMANN D., SIEKMAN D. J. Food Sci. 55(1), 95, 1990.
• KING J. W., JOHNSON J. H., FRIEDRICH J. J. Agric. Food Chem. 37, 951-954, 1989.
• KING !. W., FRANCE J., SNYDER J. M. Fresenius J. Anal. Chem. 344, 474-478, 1992.
• HAWTHORNE S. B., MILLER D. J. J. Chromatogr. Sci. 27, 197, 1989.
• GMUR W., BOSSET J. O., PLATTNER E. J. Chromatogr. 388, 335, 1987.
• SUGIYAMA K., SAITO M., HONDO T., SENDA M. J. Chromatogr. 332, 107, 1985.
• VERSCHUERE M., SANDRA P., DAVID F. J. Chromatogr. Sci. 30, 388-391, 1992.
• VERSHUERE M. PhD Thesis, Gent, Belgium, 1995.
• ALT G., HOFLER F., Proc. Second European Symposium on Analytical SFC and SFE, Riva del Garda, Italy, Eds. Sandra P. and Markides K., Huethig, Heidelberg, Germany, pp. 253-254, 1993.
• KOT A., DAVID F., SANDRA P., Proc. of the V Polish Conference on Analytical Chemistry, Gdańsk 03.09-08.09.1995. Kom. Chem. Anal. PAN - Poland, 3, 599, 1995.
• HIRATA Y., NAKATA F., HORIHATA M., J. High Resolut. Chromatogr., 11, 81, 1988.
• BUCHERL T., GRUNER A., PALIBRODA N., WOLFF E, MAPELLI G. P., Proc. Second European Symposium on Analytical SFC and SFE, Riva del Garda, Italy, Eds. Sandra P. and Markides K., Huethig, Heidelberg, Germany, pp. 87-93, 1993.
• HIRATA Y., OKAMOTO Y., J. Microcolumn Sep., 1, 46, 1989.
• JOHANSEN H. R., BECHER G., GREIBROKK T., Fressenius J. Anal. Chem., 344, 486, 1992.
• JOHANSEN H. R. THORSTENSEN C., GREIBROKK T., BECHER G., J. High Resolut. Chromatogr., 16, 148, 1993.