PL EN


Preferencje help
Widoczny [Schowaj] Abstrakt
Liczba wyników
2008 | 52 | 1 |

Tytuł artykułu

Improved analytical procedure for the determination of sulfonamides in honey

Warianty tytułu

Języki publikacji

EN

Abstrakty

EN
An improved liquid chromatography-fluorescence detection method for the determination of seven sulfonamides in bee honey was proposed. The method is selective and robust enough for the required purposes. The whole procedure was validated in accordance with the Commission Decision 657/2002/EC. Detection capabilities were from 26.15 to 49.50 µg/kg, and recoveries ranged from 32.8% to 116.1%, depending on the analyte.

Wydawca

-

Rocznik

Tom

52

Numer

1

Opis fizyczny

p.87-91,fig.,ref.

Twórcy

autor
  • National Veterinary Research Institute, 24-100 Pulawy, Poland
autor
autor

Bibliografia

  • 1. Anon.: Commission Decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. O J 2002, L 221, 8-36.
  • 2. Anon.: Council Directive 96/23/EC of 29 April 1996 on measures to monitor certain substances and residues thereof in live animals and animal products and repealing Directives 85/358/EEC, 86/469/EEC and Decision 89/187/EEC and 91/664/EEC. O J 1996, L 125, 10-31.
  • 3. Anon.: CRLs view on state of the art analytical methods for the national residues plans for control of residues. Sanco, 2006, p.3228.
  • 4. Anon.: ISO/11843: Capability of Detection (Part 1): Terms and definitions (Part 2): Methodology in the linear calibration case. International Organization for Standardization 2000.
  • 5. Berzas Nevado J.J., Castañeda Peñalvo G., Guzmán Bernardo F.J.: Simultaneous determination of sulfamethoxypiridazine, sulfamethoxazole, sulfadimethoxine and their associated compounds by liquid chromatography. Anal Chim Acta 2001, 442, 241-248.
  • 6. Berzas Nevado J.J., Castañeda Peñalvo G., Guzmán Bernardo F.J.: Simultaneous determination of sulfaquinoxaline, sulfamethazine and pyrimethazine by liquid chromatography. J Chromatogr A 2000, 870, 169- 177.
  • 7. Furusawa N.: Determining the procedure for routine residue monitoring of sulfamethazine in edible animal tissues. Biomed Chromatogr 2001, 15, 235-239.
  • 8. Gehring T.A., Rushing L.G., Thompson Jr H.C.: Determination of sulfonamides in edible salmon tissue by liquid chromatography with postcolumn derivatization and fluorescence detection. J AOAC Int 1997, 80, 751-755.
  • 9. Kaufmann A., Roth S., Ryser B., Widmer M., Guggisberg D.: Quantitative LC/MS-MS determination of sulfonamides and some other antibiotics in honey. J AOAC Int 2002, 84, 853-860.
  • 10. Kishida K., Furusawa N.: Matrix solid-phase dispersion extraction and high-performance liquid chromatographic determination of residual sulfonamides in chicken. J Chromatogr A 2001, 937, 49-55.
  • 11. Maudens K.E., Zhang G.-F., Lambert W.E.: Quantitative analysis of twelve sulfonamides in honey after acidic hydrolysis by high-performance liquid chromatography with post-column derivatization and fluorescence detection. J Chromatogr A 2004, 1047, 85-92.
  • 12. Pecorelli I., Bibi R., Fioroni L., Galarini R.: Validation of confirmatory method for the determination of sulphonamides in muscle according to the European Union regulation 2002/657/EC. J Chromatogr A 2004, 1032, 23-29.
  • 13. Posyniak A., Śniegocki T., Żmudzki J.: Solid phase extraction and liquid chromatography analysis of sulfonamide residues in honey. Bull Vet Inst Pulawy 2002, 46, 111-117.
  • 14. Posyniak A., Żmudzki J., Mitrowska K.: Dispersive solid-phase extraction for the determination of sulfonamides in chicken muscle by liquid chromatography. J Chromatogr A 2005, 1087, 259-264.
  • 15. Szymański A.: High performance liquid chromatography with micellar mobile phase in the determination of sulfonamides in honey. Chem Anal 2000, 45, 521-528.
  • 16. Verzegnassi L., Savoy-Perroud M.-C., Stadier R.H.: Application of liquid chromatography - electrospray ionization tandem mass spectrometry to the detection of 10 sulfonamides in honey. J Chromatogr A 2002, 977, 77-87.

Typ dokumentu

Bibliografia

Identyfikatory

Identyfikator YADDA

bwmeta1.element.agro-article-42ffd54a-5b16-419d-81b2-f60cb468da86
JavaScript jest wyłączony w Twojej przeglądarce internetowej. Włącz go, a następnie odśwież stronę, aby móc w pełni z niej korzystać.