Chromatographic determination of polycyclic aromatic hydrocarbons [PAH] in sewage sludge, soil, and sewage sludge-amended soils

• Autorzy: Baran S , Oleszczuk P.
• Języki publikacji: EN

Abstrakty

EN

An effective method for determining polycyclic aromatic hydrocarbons in soils fertilised with sewage sludge is presented in this paper. PAH extraction was carried out by ultrasound; dichloromethane was used as a solvent. Purification was done by means of solid phase extraction. Identification and determination was carried out by means of HPLC with a UV detector. The present analyses were carried out on the soil (control), sewage sludge, and soil fertilised with sewage sludge at a rate of 1, 2.5, 5, 10, and 20%.

Słowa kluczowe

EN

solid phase extraction; soil; ultrasonic extraction; polycyclic aromatic hydrocarbon; purification; sewage sludge; agricultural utilization; dichloromethane; methylene chloride zob.dichloromethane

• Wydawca: -
• Czasopismo: Polish Journal of Environmental Studies
• Rocznik: 2002
• Tom: 11
• Numer: 6
• Opis fizyczny: p.609-615,fig.

Twórcy

autor

Baran S

• Agricultural University, Leszczynskiego 7, 20-069 Lublin, Poland

autor

Oleszczuk P.

Bibliografia

• 1. MUNN K.J., EVANSfe CALK P.M. Mineralization of soil and legume nitrogen in soils treated with metal- contaminated sewage sludge. Soil Biol. Biochem. 32, 2031, 2000.
• 2. PETERSON A.E., SPETH P.E., SCHLECHT P. Effect of sewage sludge application on groundwater quality. [in:] Proc. of the 11th Annual Madison Waste Conf., Municipal and Industrial Waste. University of Wisconsin, Madison, WI, 1988, pp. 272.
• 3. KATTERMAN F.R.H., DAY A.D. Plant growth factors in sewage sludge. BioCycle 3, 64, 1989.
• 4. BARAN S., BIELIŃSKA J.E., WIŚNIEWSKI J. Wpływ stosowania niekonwencjonalnych nawozów wieloskładnikowych (z osadów ściekowych i wermikompostu) na wybrane właściwości gleby. Fol. Univ. Agricult. Stetin. Agricult., 72, 11, 1998.
• 5. BERSET J.D., BIGLER P., HERREN D. Analysis of nitro musk compounds and their amino metabolites in liquid sewage sludges using NMR and mass spectrometry. Anal. Chem. 72, 2124, 2000.
• 6. KIRCHMANN H., LSTROM H., JONSALL G. Organic pollutants in sewage sludge. Swedish J. Agric. Res. 21, 107, 1991.
• 7. MANGAS E., VAQUERO M.T., COMELLAS L., BROTO- PUIG F. Analysis and fate of aliphatic hydrocarbons, linear alkylbenzenes, polychlorinated biphenyls and polycyclic aromatic hydrocarbons in sewage sludge-amended soils. Chemosphere 1, 61, 1998.
• 8. MANOLI E., SAMARA C. Occurence and mass balance of polycyclic aromatic hydrocarbons in the Thessaloniki sewage treatment plant. J. Environ. Qual. 28, 176, 1999.
• 9. BODZEK D., JANOSZKA B., DOBOSZ C., WARZECHA L., BODZEK M. Determination of polycyclic aromatic compounds and heavy metals in sludges from biological sewage treatment plants. J. Chromatogr. A 774, 177, 1997.
• 10. FROST P., CAMENZIND R., MAGERT A., BONJOUR R., KARLAGANIS G. Organic micropollutants in Swiss sewage sludge. J. Chromatogr. A 643, 379, 1993.
• 11. WARZECHA L., JANOSZKA B., DOBOSZ C. Qualitative and quantitative determination of azaarenes by high­performance liquid chromatography. Chem. Anal. (Warsaw) 44, 677, 1999.
• 12. SCHNAAK W. , KUCHLER TH., KUJAWA M. , HENSCHEL K.P., SUBENBACH D., DONAU R. Organic contaminants in sewage sludge and thier exotoxicological significance in the agricultural utilization on sewage sludge. Chemosphere 1-2, 5, 1997.
• 13. YUAN S.Y., WEI S.H., CHANG B.V. Biodegradation of polycyclic aromatic hydrocarbons by a mixed culture. Chemosphere 41, 1463, 2000.
• 14. MIEGE C., DUGAY J., HENNION M.C. Optimization and validation of solvent and supercritical-fluid extractions for the trace-determination of polycyclic aromatic hydrocarbons in sewage sludges by liquid chromatography soupled to diode- array and fluorescence detection. J. Chromatogr. A 823, 219,1998.
• 15. OLESZCZUK P., BARAN S. Optimization of ultrasonic extraction of polycyclic aromatic hydrocarbons from sewage sludge samples by HPLC with UV detection accepted to Chem. Anal. (Warsaw), 2000.
• 16. LEE M.L., NOVOTNY M.V., BARTLE K.D. Analytical chemistry of polycyclic aromatic compounds, Academic Press, New York, London, Toronto, Sydney, San Francisko 1981.
• 17. TRAPIDO M. Polycyclic aromatic hydrocarbons in Estonian soil: contamination and profiles. Environ. Pollut. 105, 67, 1999.
• 18. CHEN G.S., SCHRAMM K.W., KLIMM C., XU Y., ZHANG Y.Y., KETTRUP A. Polycyclic aromatic hydrocarbons in Ya- Er Lake (Hubei, China): sources and distribution. Fresenius Z. Anal. Chem. 359, 280, 1997.
• 19. LIU M., BAUGH P.J., HUTCHINSON S.M., YU L., XU S. Historical record and sources of polycyclic aromatic hydrocarbons in core sediments from the Yangtze Estuary, China. Environ. Pollut. 110, 357, 2000.
• 20. MAXIM C.R., KOGEL-KNABNER I. Partitioning of polycyclic aromatic hydrocarbons (PAH) to water-soluble soil organic matter. Eur. J. Soil Sci. 46, 193, 1995.
• 21. MALISZEWSKA-KORDYBACH B. Trwałość wielopierścieniowych węglowodorów w glebach, IUNG Puławy 1993.
• 22. BĄKOWSKI W., JANOSZKA B. Isolation of polynuclear aromatic hydrocarbons from sewage sludges using the extraction method. Pol. J. Environ. Stud. 2, 5, 1993.
• 23. MARVIN C.H., SMITH R.W., BRYANT D.W., MCCARRY B.E. Analysis of high-molecular-mass polycyclic aromatic hydrocarbons in environmental samples using liquid chromatography atmospheric pressure chemical ionization mass spectrometry. J. Chromatogr. A 863, 13, 1999.
• 24. MITRA S., DICKHUT R.M., KUEHL S., KIMROUGH K.L. Polycyclic aromatic hydrocarbon (PAH) source, sediment deposition patterns, and particle geochemistry as factors influencing PAH distribution coefficients in sediments of the Elizabeth River, VA, USA. Mar. Chem. 66, 113, 1999.
• 25. MARCE R.M., BORRULL F. Solid-phase extraction of polycyclic aromatic compounds. J. Chromatogr. A 885, 273, 2000.
• 26. LI N., LEE H.K. Solid-phase extraction of polycyclic aromatic hydrocarbons in surface water. Negative effect of humic acid. J Chromatogr. A 921, 255, 2001.
• 27. KICINSKI H.G., ADAMEK S., KETTRUP A. Trace enrichment and HPLC analysis of polycyclic aromatic hydrocarbons in environmental samples, using solid phase extraction in connection with UV/Vis diode-array and fluorescence detection. Chromatographia 3-4, 203, 1989.
• 28. HICKS J., CORR D. Comparison of samplers to measure inhalable particulate. Ontario Ministry of the Environment, Report No ARB-40-83-ARSP, 1983.
• 29. PICHON V., BOUZIGE M., HENNION M.-C. New trends in environmental trace-analysis of organic pollutants: class- selective immunoextraction and clean-up in one step using immunosorbents. Anal. Chim. Acta 376, 21, 1998.
• 30. LEBODA R., ŁODYGA A., SIEŃKO D., GROCHOWICZ P. Adsorpcyjne metody oczyszczania i wzbogacania próbek. Wiad. Chem. 45, 217, 1991.
• 31. OLESZCZUK P., BARAN S. Application of solid-phase extraction to determination of polycyclic aromatic hydrocarbons in sewage sludge (submitted).
• 32. KISS G., VARGA-PUCHONY Z., HLAVAY J. Determination of polycyclic aromatic hydrocarbons in precipitation using solid-phase extraction and column liquid chromatography. J. Chromatogr. A 725, 261, 1996.
• 33. CONSTABLE D.J.C., SMITH R.S., TANAKA J. Comparison of solvent reduction methods for concentration of polycyclic aromatic hydrocarbon solutions. Environ. Sci. Technol. 18, 975, 1984.
• 34. FUSHENG SUN, LITTLEJOHN D., GIBSON M.D. Ultrasonication extraction and solid phase extraction clean­up for determination of US EPA 16 priority pollutant polycyclic aromatic hydrocarbons in soils by reversed-phase liquid chromatography with ultraviolet absorption detection. Anal. Chim. Acta 364, 1, 1998.
• 35. MALISZEWSKA-KORDYBACH B. Polycyclic aromatic hydrocarbons in agricultural soils in Poland - preliminary proposals for the criteria for the evaluation of the level of soils pollution. Appl. Geochem. 11, 121, 1996.
• 36. MALISZEWSKA-KORDYBACH B., SMRECZAK B. The content of polycyclic aromatic hydrocarbons (PAH) in agricultural soils in Lublin district, Roczn. Glebozn. 1-2, 95, 1997 (in Polish).
• 37. WCISŁO E. Soil contamination with polycyclic aromatic hydrocarbons (PAHs) in Poland - a review. Pol. J. Environ. Stud. 7, 267, 1998.
• 38. KUCHARSKI J., WYSZKOWSKA J., NOWAK G., HARMS H. Activity of enzymes in soils treated with sewage sludge. Pol. J. Soil Sci. 33, 29, 2000.
• 39. BECK A.J., JOHNSON D.J., JONES K.C. The form and bioavailability of non-ionic organic chemicals in sewage sludge-amended agricultural soils. Sci. Total Environ. 185, 125, 1996.
• 40. WILD S.R., WATERHOUSE K.S., MCGRATH S.P., JONES K.C. Organic contaminants in an agricultural soil with a known history of sewage sludge amended soil polynuclear aromatic hydrocarbons. Environ. Sci. Technol. 24, 1706, 1990.