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2015 | 24 | 3 |

Tytuł artykułu

Determining polybrominated diphenyl ethers in surface waters of Western Pomerania using gas chromatography with electron capture detection

Warianty tytułu

Języki publikacji

EN

Abstrakty

EN
We show how to determine polybrominated diphenyl ethers in aqueous samples using liquid-liquid extraction and gas chromatography with electron capture detection (LLE-GC-μECD). This method, due to its simplicity, low limits of determination (7-9 pg/L), high accuracy, relatively low costs, and high recovery coefficients for all of these PBDEs (86-92%), offers enormous benefits for routine analyses of PBDEs. The developed method was applied to surface water samples collected from different sampling points in western Pomerania.

Słowa kluczowe

Wydawca

-

Rocznik

Tom

24

Numer

3

Opis fizyczny

p.961-968,fig.,ref.

Twórcy

  • Institute of Chemistry and Environmental Protection, West Pomeranian University of Technology, Al.Piastow 42, 71-065 Szczecin, Poland
autor
  • Institute of Chemistry and Environmental Protection, West Pomeranian University of Technology, Al.Piastow 42, 71-065 Szczecin, Poland

Bibliografia

  • 1. ĆWIKLAK K., JABŁOŃSKA M. Polybrominated diphenyl ethers in the environment. Laboratorium 9/2008, 10-14, 2008 [In Polish]
  • 2. FULARA I., CZAPLICKA M. Methods for determination of polybrominated diphenyl ethers in environment al samples – review. J. Sep. Sci. 35, 2075, 2012.
  • 3. MONTES R., RODRIGUEZ I., RUBI E., CELA R. Suitability of polydimethylsiloxane rods for the headspace sorptive extraction of polybrominated diphenyl ethers from water samples. J. Chromatogr. A, 1143, 41, 2007.
  • 4. DASO A. P., FATOKI O.S., ODENDAAL J. P. Occurrence of polybrominated diphenyl ethers (PBDEs) and 2,2’,4,4’,5,5’-hexabromobiphenyl (BB-153) in water samples from the Diep River, Cape Town, South Africa. Environ Sci Pollut Res, 20, 5268, 2013.
  • 5. HERNIK A., GÓRALCZYK K., CZAJA K., STRUCIŃSKI P. I LUDWICKI W. Polybrominated diphenyl ethers (PBDEs) – new danger? Roczn. PZN 58, (2), 403, 2007 [In Polish].
  • 6. GÓRALCZYK K., STRUCIŃSKI P., CZAJA K., HERNIK A. I LUDWICKI J.K. Flame retardants – the use and danger to human. Roczn. PZH 53, (3), 293, 2002 [In Polish]
  • 7. RAHMAN F., LANGFORD K.H., SCRIMSHAW M.D. I LESTER J.N. Polybrominated diphenyl ether PBDE flame retardants. Sci. Total Environ. 275, 1, 2001.
  • 8. de WIT C. An overview of brominated flame retardants in the environment. Chemosphere 46, 583, 2002.
  • 9. FONTANALS N., BARRI T., BERGSTOM S., JONSSON JA. Determination of polybrominated diphenyl ethers at trace levels In enironmental Walters using hollow-fiber microporous membrane liquid-liquid extraction and gas chromatography-mass spectrometry. J. Chromatogr. A 1133, 41, 2006.
  • 10. FONTANA A.R., WUILLOUD R.G., MARTINEZ L.D., ALTAMIRANO J.C. Simple approach based on ultrasoundassisted emulsification-microextraction for determination of polybrominated flame retardants in water samples by gas chromatography-mass spectrometry. J. Chromatogr. A 1216, 147, 2009.
  • 11. BACALONI A., CALLIPO L., CORRADINI E., GIANSANTI P., GUBBIOTTI R., SAMPERI R., LAGANA A. Liquid chromatography-negative ion atmospheric pressure photoionization tandem mass spectrometry for the determination of brominated flame retardants in environmental water and industrial effluents. J. Chromatogr. A 1216, 6400, 2009.
  • 12. FONTANA A.R., SILVA M.F., MARTINEZ L.D., WUILLOUD R.G., ALTAMIRANO J.C. Determination of polybrominated diphenyl ethers in water and soil samples by cloud point extraction-ultrasound-assisted back-extractiongas chromatography-mass spectrometry. J. Chromatogr. A 1216, 4339, 2009.
  • 13. LIU X., LI J., ZHAO Z., ZHANG W., LIN K., HUANG C., WANG X. Solid-phase extraction combined with dispersive liquid-liquid microextraction for the determination for polybrominated diphenyl ethers In different enironmental matrices. J. Chromatogr. A 1216, 2220, 2009.
  • 14. SUN J., LIU J., LIU Q., QU G., RUAN T., JIANG G. Sample preparation method for the speciation of polybrominated diphenyl ethers and their methoxylated and hydroxylated analogues in diverse environmental matrices. Talanta 88, 669, 2012.
  • 15. ZHAO R., LIU Y., CHEN X., YUAN J., BAI A., ZHOU J. Preconcentration and determination of polybrominated diphenyl ethers in environmental water samples by solidphase microextraction with Fe₃O₄-coated bamboo charcoal fibers prior to gas chromatography-mass spectrometry. Anal. Chim. Acta 769, 65, 2013.
  • 16. CHEN X., CHENG C., WANG X., ZHAO R. Sensitive determination of polybrominated diphenyl ethers in environmental water samples with etched stainless steel wire based on solid-phase microextraction prior to gas chromatography-mass spectrometry. Anal. Methods 4, 2908, 2012.
  • 17. ZHAO A., WANG X., MA M., WANG W., SUN H., YAN Z., XU Z., WANG H. Tempereture-assisted ionic liquid dispersive liquid-liquid microextraction combined with high performance liquid chromatography for the determination of PCBs and PBDEs in water and urine samples. Microchim Acta 177, 229, 2012.
  • 18. LI Y., WEI G., HU J., LIU X., ZHAO X., WANG X. Dispersive liquid-liquid microextraction followed by reversed phase-high performance liquid chromatography for the determination of polybrominated diphenyl ethers at trace levels in landfill leachate and environmental water samples. Anal. Chim. Acta 615, 96, 2008.
  • 19. ZHANG Q., LIANG T., GUAN L. Ultrasound-assisted dispersive liquid–liquid microextraction combined with gas chromatography-mass spectrometry in negative chemical ionization mode for the determination of polybrominated diphenyl ethers in water. J. Sep. Sci. 36, 1263, 2013.

Typ dokumentu

Bibliografia

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Identyfikator YADDA

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