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Z-RNA. The synthesis of 2'-O-[13C]methyl- and 5-methyl-analogs of ribo-CGCGCG

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Biala E., Milecki J., Kowalewski A., Popenda M., Antkowiak W. Z., Adamiak R. W.

Acta Biochimica Polonica

1993

tom 40

nr 4

Chemical synthesis of 2'-0-[13C methyl-rCGCGCG and 5-methyl-rCGCGCG using support-aided phosphoramidite method is presented. 2'-0-Methyl guanosine derivative was separated from its 3'-0-methyl counterpart using transient 5',3'-0-silylation with l,3-dichloro-l,l,3,3-tetraisopropyldisiloxane (Markiewicz reagent). The hexamers were obtained in a purity suitable for NMR studies.

Ograniczanie wyników

1 Acta Biochimica Polonica

1 Adamiak R. W.

1 Antkowiak W. Z.

1 Biala E.

1 Kowalewski A.

1 Milecki J.

1 Popenda M.

1 1993

Wyniki wyszukiwania

Z-RNA. The synthesis of 2'-O-[13C]methyl- and 5-methyl-analogs of ribo-CGCGCG