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2010 | 54 | 3 |

Tytuł artykułu

Simple method to determine of sulfonamides in muscles by high performance liquid chromatography

Warianty tytułu

Języki publikacji

EN

Abstrakty

EN
A sensitive and selective LC method has been developed for the simultaneous determination of ten sulfonamides in muscles, after pre-column derivatization with fluorescamine. The whole procedure was validated in accordance with the Commission Decision 2002/657/EC. Detections capabilities (CCß) were from 125 µg/kg to 150 µg/kg, and recoveries ranged from 60% to 100% pending from analyte. The results demonstrate that the LC-FLD system is highly effective in analysing trace sulfonamides in muscles.

Wydawca

-

Rocznik

Tom

54

Numer

3

Opis fizyczny

p.393-396,fig.,ref.

Twórcy

  • Department of Pharmacology and Toxicology, National Veterinary Research Institute, 24-100 Pulawy, Poland
autor

Bibliografia

  • 1. Berzas N., Castañeda P., Guzmán B.: Simultaneous determination of sulfamethoxypiridazine, sulfamethoxazole, sulfadimethoxine and their associated compounds by liquid chromatography. Anal Chim Acta 2001, 442, 241-248.
  • 2. Berzas N., Castañeda P., Guzmán B.: Simultaneous determination of sulfaquinoxaline, sulfamethazine and pyrimethazine by liquid chromatography. J Chromatogr A 2000, 870, 169-177.
  • 3. European Commission Decision of August 2002 2002/657/EC implementing Council Directive 96/23/EC.
  • 4. European Commission Regulation No. 2377/1990. Off J Eur Commun 1990, L224, 1-43.
  • 5. Furusawa N.: Determining the procedure for routine residue monitoring of sulfamethazine in edible animal tissues. Biomed Chromatogr 2001, 15, 235-239.
  • 6. Furusawa N., Kishida K.: Matrix solid-phase dispersion extraction and high-performance liquid chromatographic determination of residual sulfonamides in chicken. J Chromatogr A 2001, 937, 49-55.
  • 7. Gehring T., Rushing L., Thompson H.: Determination of sulfonamides in edible salmon tissue by liquid chromatography with post column derivatization and fluorescence detection. J AOAC Int 1997, 4, 80.
  • 8. Hanwen S., Lianfeng A., Fengchi W.: Quantitative analysis of sulfonamide residues in natural animal casings by HPLC. Chromatographia 2007, 66, 333-337.
  • 9. Hela W., Brandtner M., Widek R., Schuh R.: Determination of sulfonamides in animal tissues using cation exchange reversed phase sorbent for sample cleanup and HPLC-DAD for detection. Food Chem 2003, 83, 601-608.
  • 10. Jacobsen A. M., Halling-Sørensen B.: Multi-component analysis of tetracyclines, sulfonamides and tylosin in swine manure by liquid chromatography-tandem mass spectrometry. Anal Bioanal Chem 2006, 384, 1164- 1174.
  • 11. Pecorelli I., Bibi R., Fioroni L., Galarini R.: Validation of confirmatory method for the determination of sulphonamides in muscle according to the European Union regulation 2002/657/EC. J Chromatogr A 2004, 1032, 23-29.
  • 12. Perret D., Gentili A., Marchese S., Greco A., Curini R.: Sulphonamide residues in Italian surface and drinking waters: a small scale reconnaissance. Chromatographia 2006, 63, 225-232.
  • 13. Posyniak A., Zmudzki J., Mitrowska K.: Dispersive solid-phase extraction for the determination of sulfonamides in chicken muscle by liquid chromatography. J Chromatogr A 2005, 1087, 259-264.
  • 14. Tarbin J. A., Clarke P., Shearer G.: Screening of sulphonamides in egg using gas chromatography - mass selective detection and liquid chromatography-mass spectrometry. J Chromatogr B 1999, 729, 127-138.
  • 15. Zengxuan C., Yu Z., Hongfeng P., Xiaowei T., Yiping R.: Simultaneous determination of 24 sulfonamide residues in meat by ultra-performance liquid chromatography tandem mass spectrometry. J Chromatogr A 2008, 1200, 144-155.
  • 16. Zotou A., Vasiliadou Ch.: A fluorescence-LC method for the determination of sulfonamides in biological fluids with pre-column derivatization. Chromatographia 2009, 70, 389-397.

Typ dokumentu

Bibliografia

Identyfikatory

Identyfikator YADDA

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