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2013 | 22 | 5 |

Tytuł artykułu

Determining PCBs in fish and sediment samples related to intercomparison studies

Autorzy

Warianty tytułu

Języki publikacji

EN

Abstrakty

EN
This paper reports on the analysis of polychlorinated biphenyls (PCBs) in selected intercomparison materials (IAEA-435 (tuna) and IAEA-159 (sediment)), and presents the author’s results against the background of results accepted by the organizer of the intercomparison studies, i.e. the Marine Environment Laboratories of the International Atomic Energy Agency in Monaco. The samples were extracted with a mixture of acetone/hexane (tuna) or acetonitrile (sediment) by sonication, cleaned up using micro-columns packed with different materials (e.g. silica gel, florisil, copper), and analyzed by GC-ECD. The difficulties of PCB determination are indicated and the differences between the analyses of low- and high-molecular-weight PCBs are emphasized.

Wydawca

-

Rocznik

Tom

22

Numer

5

Opis fizyczny

p.1341-1347,fig.,ref.

Twórcy

  • Marine Pollution Laboratory, Institute of Oceanology, Polish Academy of Sciences, Powstancow Warszawy 55, 81-712 Sopot, Poland

Bibliografia

  • 1. Stockholm Convention on Persistent Organic Pollutants, http://chm.pops.int/Convention/ConventionText/tabid/2232/ Default.aspx, 2009.
  • 2. Scientific Report of EFSA – Results of the monitoring of non dioxin-like PCBs in food and feed, EFSA Journal, 8, (7), 170, http://www.efsa.europa.eu/de/efsajournal/doc/1701.pdf, 2010.
  • 3. HELCOM, Hazardous substances in the Baltic Sea – An Integrated Thematic Assessment of Hazardous Substances in the Baltic Sea, Balt. Sea Environ. Proc. 120B, 2010.
  • 4. OSPAR Commission, Status and Trend in Marine Chemical Pollution, http://qsr2010.ospar.org/media/assessments/p00395_Chemical_status_and_trend_HA-6.pdf, 2009.
  • 5. MUIR D., SVERKO E. Analytical methods for PCBs and organochlorine pesticides in environmental monitoring and surveillance: a critical appraisal. Anal. Bioanal. Chem. 386, 769, 2006.
  • 6. VILLENEUVE J.-P., De MORA S.J., CATTINI C. Worldwide and regional intercomparison for the determination of organochlorine compounds and petroleum hydrocarbons in tuna homogenate IAEA-435. International Atomic Energy Agency, Marine Environment Laboratory, Report No. 78, 2006.
  • 7. VILLENEUVE J.-P., OH J.R., CATTINI C. World-wide and regional intercomparison for the determination of organochlorine compounds, petroleum hydrocarbons and sterols in the sediment sample IAEA-159. International Atomic Energy Agency, Marine Environment Laboratories, Report No. 80, 2007.
  • 8. KOWALEWSKA G., KONAT J. Determination of polychlorinated biphenyls in the marine sediments using gas chromatography. Chem. Anal. (Warsaw) 44, 223, 1999.
  • 9. KONAT J., KOWALEWSKA G. Polychlorinated biphenyls (PCBs) in sediments of the southern Baltic Sea – trends and fate. Sci. Total Environ. 280, 1, 2001.
  • 10. LANG V. Polychlorinated biphenyls in the environment. J. Chromatogr. 595, 1, 1992.
  • 11. SKARPHEDINSDOTTIR H., GUNNARSSON K., GUDMUNDSSON G.A., NFON E. Bioaccumulation and Biomagnification of Organochlorines in a Marine Food Web at a Pristine Site in Iceland. Arch. Environ. Con. Tox. 58, 800, 2010.
  • 12. De BOER J., WELLS D.E. Chlorobiphenyls and organochlorine pesticides in fish and sediments – three years of QUASIMEME Laboratory Performance Studies. Mar. Pollut. Bull. 35, 52, 1997.
  • 13. BLANZ T., SCHULZ-BULL D.E., EMEIS K.C., PETRICK G., DUINKER J.C. Chlorobiphenyls in suspension and sediment of the southern Baltic Sea: a mass balance calculation since the onset of PCB-production. Cont. Shelf Res. 19, 891, 1999.
  • 14. SCHULZ-BULL D.E., PETRICK G., KANNAN N., DUINKER J.C. Distribution of individual chlorobiphenyls (PCB) in solution and suspension in the Baltic Sea. Mar. Chem. 48, 245, 1995.
  • 15. THOMPSON M., WOOD R. The international harmonized protocol for the proficiency testing of (chemical) analytical laboratories. Pure Appl. Chem. 65, 2123, 1993.
  • 16. CLEEMANN M., RIGET F., PAULSEN G.B., KLUNGSØYR J., DIETZ R. Organochlorines in Greenland marine fish, mussels and sediments. Sci. Total Environ. 245, 87, 2000.
  • 17. STEPHANSEN D. A., SVENDSEN T. C., VORKAMP K., FRIER J.-O. Changes in patterns of persistent halogenated compounds through a pelagic food web in the Baltic Sea. Mar. Environ. Res. 73, 17, 2012.
  • 18. HELGASON L.B., BARRETT R., LIE E., POLDER A., SKAARE J.U., GABRIELSEN G.W. Levels and temporal trends (1983-2003) of persistent organic pollutants (POPs) and mercury (Hg) in seabird eggs from Northern Norway. Environ. Pollut. 155, 190, 2008.
  • 19. HILLER E., ZEMANOVÁ L., SIROTIAK M., JURKOVIĆ L. Concentrations, distributions, and sources of polychlorinated biphenyls and polycyclic aromatic hydrocarbons in bed sediments of the water reservoirs in Slovakia. Environ. Monit. Assess. 173, 883, 2011.
  • 20. THOMPSON S., BUDZINSKI H., LEMENACH K., LETELLIER M., GARRIGUES P. Multi-residue analysis of polycyclic aromatic hydrocarbons, polychlorobiphenyls, and organochlorine pesticides in marine sediments. Anal. Bioanal. Chem. 372, 196, 2002.
  • 21. HONG Y., YU S., YU G., LIU Y., LI G., WANG M. Impacts of urbanization on surface sediment quality: evidence from polycyclic aromatic hydrocarbons (PAHs) and polychlorinated biphenyls (PCBs) contaminations in the Grand Canal of China. Environ. Sci. Pollut. Res. 19, 1352, 2012.
  • 22. FILIPKOWSKA A., LUBECKI L., KOWALEWSKA G. Polycyclic aromatic hydrocarbon analysis in different matrices of the marine environment. Anal. Chim. Acta 547, 243, 2005.
  • 23. WOLSKA L., RAWA-ADKONIS M., NAMIEŚNIK J. Determining PAHs and PCBs in aqueous samples: finding and evaluating sources of error. Anal. Bioanal. Chem. 382, 1389, 2005.
  • 24. KOWALEWSKA G., KONAT J., DOBROWOLSKA Ś. Why is it easier to determine PAHs than PCBs in marine sediments? Chem. Anal. (Warsaw) 47, 189, 2002.

Typ dokumentu

Bibliografia

Identyfikatory

Identyfikator YADDA

bwmeta1.element.agro-ec2e0eee-a6b9-4d5a-9235-c78a9bcc2537
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