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2011 | 55 | 4 |

Tytuł artykułu

Multi-class procedure for analysis of antibacterial compounds in animal tissues by liquid chromatography-tandem mass spectrometry

Warianty tytułu

Języki publikacji

EN

Abstrakty

EN
A liquid chromatographic method coupled with tandem mass spectrometry for the determination of residues of β-lactams, macrolides, tetracyclines, quinolones, sulfonamides, aminoglycosides, and lincosamides in animal tissues was described. Analytes were isolated from biological material with acetonitrile or with trichloroacetic acid. The procedure was validated according to European Decision 2002/657/EC.

Słowa kluczowe

Wydawca

-

Rocznik

Tom

55

Numer

4

Opis fizyczny

p.741-748,fig.,ref.

Twórcy

autor
  • Department of Pharmacology and Toxicology, National Veterinary Research Institute, 24-100 Pulawy, Poland
autor
autor
autor
autor

Bibliografia

  • 1. Alfredsson G., Branzell C., Granelli K., Lundstrom A.: Simple and rapid screening and confirmation of tetracyclines in honey and egg by a dipstick test and LC-MS/MS. Anal Chim Acta 2005, 529, 47-51.
  • 2. Babin Y., Fortier S.: A high-throughput analytical method for determination of aminoglycosides in veal tissues by liquid chromatography/tandem mass spectrometry with automated cleanup. J AOAC Int 2007, 90, 1418-1426.
  • 3. Bailac S., Barron D., Barbosa J.: New extraction procedure to improve the determination of quinolones in poultry muscle by liquid chromatography with ultraviolet and mass spectrometric detection. Anal Chim Acta 2006, 580, 163-169.
  • 4. Becker M., Zittlau E., Petz M.: Residue analysis of 15 penicillins and cephalosporins in bovine muscle, kidney and milk by liquid chromatography-tandem mass spectrometry. Anal Chim Acta 2004, 520, 19-32.
  • 5. Berrada H., Borrull F., Font G., Molto J.C., Marce R.M.: Validation of a confirmatory method for the determination of macrolides in liver and kidney animal tissues in accordance with the European Union regulation 2002/657/EC. J Chromatogr A 2007, 1157, 281-288.
  • 6. Cantwell H., O’Keefee M.: Evaluation of the Premi Test and comparison with the One-Plate Test for the detection of antimicrobials in kidney. Food Add Contam 2006, 23, 120-125.
  • 7. Cherlet M., Schelkens M., Croubels S., De Backer P.: Quantitative multi-residue analysis of tetracyclines and their 4-epimers in pig tissues by high-performance liquid chromatography combined with positive-ion electrospray ionization mass spectrometry. Anal Chim Acta 2003, 492, 199-213.
  • 8. Chico J., Rubies A., Centrich F., Campanyo R., Prat M.D., Granados M.: High-throughput multiclass method for antibiotics residue analysis by liquid chromatography-tandem mass spectrometry. J Chromatogr A 2008, 1213, 189-199.
  • 9. Codony R., Compano R., Granados M., Garcia-Regueiro J.A., Prat M.D.: Residue analysis of macrolides in poultry muscle by liquid chromatography-electrospray mass spectrometry . J Chromatogr A 2002, 959, 131-141.
  • 10. Commission Decision 2002/657/EC of August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Off J Eur Commun 2002, L 221, 8-36.
  • 11. Commission Regulation (UE) 37/2010 of 22nd December 2009 on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin. Off J Eur Commun 2010, L 15, 1-72.
  • 12. Council Directive 96/23/EC of April 1996 on measures to monitor certain substances and residues thereof in live animals and animal products and repealing Directives 85/358/EEC and 86/469/EEC and Decisions 89/18/EEC and 91/664/EEC. Off J Eur Commun 1996, L 125, 10-32.
  • 13. Di Sabatino M., Di Pietra A.M., Benfenati L., Di Simone B.: Determination of 10 sulfonamide residues in meat samples by liquid chromatography with ultraviolet detection. J AOAC Int 2009, 90, 598-603.
  • 14. Gaugain-Juhel M, Anger B., Laurentie M.: Multiresidue chromatographic method for the determination of macrolide residues in muscle by high-performance liquid chromatography with UV detection. J AOAC Int 1999, 82, 1046-1053.
  • 15. Gaugain-Juhel M., Delepine B., Gautier S., Fourmond M.P., Gaudin V., Hurtaud-Pessel D., Verdon E., Sanders P.: Validation of liquid chromatography-tandem mass spectrometry screening method to monitor 58 antibiotics in milk: a qualitative approach. Food Add Contam 2009, 26, 1459-1471.
  • 16. Granelli K., Branzell C.: Rapid multi-residue screening of antibiotics in muscle and kidney by liquid chromatography-electrospray ionization-tandem mass spectrometry. Anal Chim Acta 2007, 586, 289-295.
  • 17. Heller D.N., Ngoh M.A., Donoghue D., Podhorniak L., Righter H., Thomas M.H.: Identification of incurred sulfonamide residues in eggs: method confirmation by liquid chromatography-tandem mass spectrometry and quantitation by liquid chromatography with ultraviolet detection. J Chomatogr В 2002, 774, 39-52.
  • 18. Holthoon van F.L., Essers M.L., Mulder P.J., Stead S.L., Caldow M., Ashwin H.M., Sharman M.: A generic method for the quantitative analysis of aminoglycosides (and spectinomycin) in animal tissue using methylated internal standards and liquid chromatography tandem mass spectrometry. Anal Chim Acta 2009, 637, 135-143.
  • 19. Kaufmann A., Butcher P., Maden K., Widmer M.: Quantitative multiresidue method for about 100 veterinary drugs in different meat matrices by sub 2-µm particulate high-performance liquid chromatography coupled to time of flight mass spectrometry. J Chromatogr A 2008, 1194, 66-79.
  • 20. Martos P.A., Jayasundara F., Dolbeer J., Jin W., Spilsbury L., Mitchell M., Varilla C., Shurmer B.: Multiclass, multiresidue drug analysis, including aminoglycosides, in animal tissue using liquid chromatography coupled to tandem mass spectrometry. J Agic Food Chem 2010, 58, 5932-5944.
  • 21. McGrath T., Baxter A., Ferguson J., Haughey S., Bjurling P.: Multi sulfonamide screening in porcine muscle using a surface plasmon resonance biosensor. Anal Chim Acta 2005, 529, 123-127.
  • 22. Msagati T.A.M., Nindi M.M.: Determination of β-lactam residues in foodstuffs of animal origin using supported liquid membrane extraction and liquid chromatography - mass spectrometry. Food Chem 2007, 100, 836-844.
  • 23. Posyniak A., Zmudzki J., Ellis R.L., Semeniuk S., Niedzielska J.: Determination of fluoroquinolone residues in animal tissues by liquid chromatography. Biomed Chromatogr 1999, 13, 279-285.
  • 24. Posyniak A., Zmudzki J., Mitrowska K.: Dispersive solid-phase extraction for the determination of sulfonamides in chicken muscle by liquid chromatography. J Chromatogr A 2005,1087, 259-264.
  • 25. Romero-Gonzalez R., Lopez-Martinez J.C., Gomez-Milan E., Garrido-Frenich A., Martinez-Vidal J.L.: Simultaneous determination of selected veterinary antibiotics in gilthead seabream (Sparus aurata) by liquid chromatography-mass spectrometry. J Chromatogr В 2007, 857, 142-148.
  • 26. Stead S., Sharman M., Tarbin J.A., Gibson E., Richmond S., Stark J., Geijp E.: Meeting maximum residue limits: an improved screening technique for the rapid detection of antimicrobial residues in animal food products. Food Add Contam 2004, 21, 216-221.

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Typ dokumentu

Bibliografia

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