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2007 | 51 | 3 |

Tytuł artykułu

Comparison of microbiological plate-four level assay and liquid chromatography analysis for the determination of amoxicillin in medicated feedingstuff

Warianty tytułu

Języki publikacji

EN

Abstrakty

EN
The experiment was purposed to compare amoxicillin determination in medicated feedingstuff by a microbiological method (microbiological plate-four level test) and a liquid chromatography with fluorescence detection (LC- FLD) with pre-column derivatisation with formaldehyde. Amoxicillin was determined in the medicated feedingstuff at the level of 250 mg/kg. The results indicated that the microbiological method might provide adequate data suitable for amoxicillin determination in the medicated feedingstuff. These results were confirmed by the LC method. Therefore, for practical use, the values obtained with two methods can be considered equivalent.

Wydawca

-

Rocznik

Tom

51

Numer

3

Opis fizyczny

p.393-396,fig.,ref.

Twórcy

  • National Veterinary Research Institute, 24-100 Pulawy, Poland
autor

Bibliografia

  • 1. Catharina Y.W., Luo W.: A bridging study between liquid chromatography and microbial inhibition assay methods for determining amoxicillin residues in catfish muscle. J AOAC 1998, 81, 33-39.
  • 2. Council Directive of 26 March 1990 laying down the conditions governing the preparation, placing on the market and use of medicated feedingstuffs in the Community (90/167/EWG) (OJ No. L 87 2.4.92 p.37).
  • 3. Coutting J., Harlbut J., Sofos J.: Quantitation of penicillin G in medicated premix feed by micellar electrokinetic capillary chromatography. J AOAC Int 1997, 80, 951-955.
  • 4. De Baere S., De Backer P.: Quantitative determination of amoxicillin in animal feed using liquid chromatography with tandem mass spectrometric detection. Anal Chim Acta 2007, 586, 319-325.
  • 5. Douša M., Hosmanová R.: Rapid determination of amoxicillin in premixes by HPLC. J Pharm Biomed Anal 2005, 37, 373-377.
  • 6. Gamba V., Dusi G.: Liquid chromatography with fluorescence detection of amoxicillin and ampicillin in feed using pre-column derivatization. Anal Chim Acta 2003, 483, 69-72.
  • 7. LaCourse W., Dasenbrock C.: Pulsed electrochemical detection of sulphur-containing antibiotics following high performance liquid chromatography. J Pharm Biomed Anal 1999, 19, 239-252.
  • 8. Lohajova L., Nagy J., Różańska H., Popelka P., Jevinova P.: Suitability of STAR and PREMI®test for the detection of amoxicillin residue in laying hens. Bull Vet Inst Pulawy 2006, 50, 367-371.
  • 9. Lott A., Smither R., Vaughan D.: Antibiotic identification by high voltage electrophoresis bioautography. J Assoc Anal Chem 1985, 68, 1018-1020.
  • 10. Pérez-Lozano P., García-Montoya A., Orriols A., Miñarro M., Ticó J. R., Suñé-Negre J. M.: Stability evaluation of amoxicillin in a solid premix veterinary formulation by monitoring the degradation products through a new HPLC analytical method. J Pharm Biomed Anal 2006, 42, 192-199.
  • 11. Polish Pharmacopoeia, 2002, Edition VI, pp. 131-141.

Typ dokumentu

Bibliografia

Identyfikatory

Identyfikator YADDA

bwmeta1.element.agro-article-d81f730c-052b-432a-a7eb-b0f2c512c455
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