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1996 | 05 | 5 |
Tytuł artykułu

Determination of beta-agonists in biological samples by thin layer and liquid chromatographic methods

Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
A simple and sensitive method for the determination of ß-agonists in animal tissue and urine using thin layer and liquid chromatography was prepared. The development of the method involves optimization of sample clean-up (solid-phase extraction) and chromatographic separation and detection conditions. The recovery of salbutamol and clenbuterol from tissue and urine samples were above 80% and the limit of detection was 1 ng g-1. The method has been used on a routine scale for residue control in samples from meat-producing animals.
Wydawca
-
Rocznik
Tom
05
Numer
5
Opis fizyczny
p.33-36,fig.,ref.
Twórcy
autor
  • National Veterinary Research Institute, Partyzantow 57, 24-100 Pulawy, Poland
autor
autor
Bibliografia
  • DALRYMPLE R.H., BAKER R.K., GINGHER D.E., INGLE D.L., PENSACK J.M., RICKS C.A. A Repartinioning Agent to Improve Performance and Carcass Composition of Broilers. Poult. Sci., 63, 2376-2380, 1984.
  • MILLER M.F., GARCIA D.K., COLEMAN M.E., EKEREN P.A., LUNT D.K., WAGNER K.A., PROCKNOR M.,
  • WELSH T.H., SMITH S.B. Adipose Tissue, Longissimus Muscle and Anterior Pituarity Growth and Function in Clenbuterolfed Heifers. J. Anim. Sci., 66, 12-16, 1988.
  • MARTINEZ-NAVARRO J.F. Food Poisoning Related to the Consumption of Illicit Beta-agonist in Livers. Lancet, 336, 1311, 1990.
  • PULCE C., LAMAISON D., KECK G., BOSTVIRONNAIS C., NICOLAS J., DESCOTES J. Collective Human Food Poisoning by Clenbuterol Residues in Veal Liver. Vet. and Hum. Toxicol., 33, 480-481, 1991.
  • DEGAND G., BERNES-DUYCKAERTS A., MAGHUIN-ROGISTER G. Determination of Clenbuterol in Bovine Tissues and Urine by Enzyme Immunoassay. ]. Of Agric. Food Chem., 40, 70-74, 1992.
  • PICKETT R.J.H., SAUER M.]. Determination of Clenbuterol in Bovine Urine by Enzyme Immunoassay Following Concentration and Clean-up by Immunoaffinity Chromatography. Anal. Chim. Acta, 275, 269-273, 1993.
  • COURTHEYN D., DESAEVER C., VERHE R. High-performance Liquid Chromatographic Determination of Clenbuterol l and Cimaterol Using Postcolumn Derivatization. J. Chromatogr., 564, 537-548, 1991.
  • HOOIJERINK H., SCHILT R., HAASNOOT W., COURTHEIJN D. Determination of Clenbuterol in Urine of Calves by High-performance Liquid Chromatography with in Series Ultrafiolet and Electrochemical Detection. J. Pharm. Biomed. Anal, 9, 485-492, 1991.
  • WILSON R.T., GRONECK J.M., HOLLAND K.P., HENRY A.C. Determination of Clenbuterol in Cattle, Sheep, and Swine Tissues by Electron Ionzation Gas Chromatography/Mass Spectrometry. J. AOAC. Int., 77, 917 -924, 1994.
  • FURST P., FURST CH., GROEBEL W. GC/MS-Bestimmung von Clenbuterol in Lebensmitteln, Futtermitteln und Urin. Dstch. Lebensm.-Rundsch., 85, 35-39, 1989.
  • DEGROODT J.M., WYHOWSKI DE BUKANSKI B., BEERNAERT H., COURTHEYN D. Clenbuterol Residue Analysis by HPLC-HPTLC in Urine and Animal Tissues. Z. Lebensm. Unters. Forsch. 189, 128-131, 1989.
  • SCHMITZ P., DEGANTD G., PELZER G., GASPAR P., MAGHUIN-ROGISTER G. Developpements analytiques pour la detection du clenbuterol utilise comme agent de repartition de graisse chez les animaux de boucherie. Ann. Med. Vet., 133, 427-430, 1989.
  • POSYNIAK A., NIEDZIELSKA J., SEMENIUK S., ŻMUDZKI J. Screening for Clenbuterol and Salbutamol Residues in Urine by Planar Chromatography. J. Planar Chromatogr., 8, 157-159, 1995.
  • SCHEURER J., MOORE CH.M., Solid-phase Extraction of Drugs from Biological Tissues-a Review. J. Anal. Toxicol., 16, 264-269, 1992.
  • KRISHNAN T.R., IBRAHAM I. Solid-phase Extraction Technique for the Analysis of Biological Samples. J. Pharm. Biomed. Anal, 12, 287-293, 1994.
Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.agro-article-a72dc05a-17a0-4848-8f5d-1871780decf2
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