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2008 | 17 | 5 |

Tytuł artykułu

Speciation analysis of lead, zinc and cadmium in river bottom deposits in Swietokrzyskie Region

Autorzy

Warianty tytułu

Języki publikacji

EN

Abstrakty

EN
Bottom deposits of selected rivers in the Świętokrzyskie Region of Poland flowing through areas of various geological characteristics and land development were analyzed for the presence of cadmium, zinc and lead. Microwave-assisted 3-stage sequential extraction recommended by the European Union (EU) was applied for that purpose as well as a 5-stage extraction proposed by Tessier et al. Residues after sequential extraction were mineralized in concentrated nitric acid in order to check if applied sequential extraction procedures allowed extraction of total amounts of metals from bottom deposits. Metal contents were determined with F-AAS technique in particular extracts.

Wydawca

-

Rocznik

Tom

17

Numer

5

Opis fizyczny

p.781-789,fig.,ref.

Twórcy

autor
  • Jan Kochanowski University of Humanic and Natural Science in Kielce, Swietokrzyska Str.15, 25-406 Kielce, Poland

Bibliografia

  • 1. BIERŁA K., SIEPAK J. Heavy Metals in Bottom Sediments from the Odra River. in: Młodzi chemicy - rocznik 2003, Wydz. Chem. UAM, pp. 25-28, 2003 [In Polish].
  • 2. GŁOSIŃSKA G., SIEPAK J. Heavy metals in floodplain. Ekologia 3 (35), 36, 2006 [In Polish].
  • 3. NEYA R. Metallic material – zinc, lead. Polska Akademia Nauk, Kraków, pp. 194-197, 1997 [In Polish].
  • 4. WALLING D.E., OWENS P.N. The role of overbank floodplain sedimentation in catchment contaminant budgets. Hydrobiologia 494, 83, 2003.
  • 5. MILLER J.R. The role of fluvial geomorphic processes in the dispersal of heavy metals from mine sites. J. Geochem. Explor. 58, 101, 1997.
  • 6. HELIOS-RYBICKA E. The parameters determining a distribution of heavy metals in water – sediment system. Geochemical. hydrogeochemical and biochemical environmental change in anthropogenic region. Materials of IX Scientific Conference AGH – Kraków, 1997 [In Polish].
  • 7. SOBCZYŃSKI T., SIEPAK J. Speciation of heavy metals in like sediments in: Speciation analyses of heavy metals in waters and sediments samples. UAM, Poznań, 1998 [In Polish].
  • 8. DAWSON E.J., MACKLIN M.G. Speciation of heavy metals in floodplain and food sediments: a reconnaissance survey of the Air Valley. West Yorkshire, Great Britain, Environ. Geoche¬m. Hlth. 20, 67, 1998.
  • 9. LOPEZ-SANCHEZ J.F., SAHUQUILLO A., RAURET G., LACHICA M., GOMEZ A., URE A.M., MUNTAU H., QUEVAUVILLER Ph. Extraction procedures for soil analysis. in: Quevauviller Ph. (Eds.) Methodologies for soil and sediment fractionation studies. The Royal Society of Chemistry, Cambridge UK, pp. 1-9, 2002.
  • 10. SNAPE I., SCOULLER R.C., STARK S.C., STARK J., RIDDLE M.J., GORE D.B. Characterisation of the dilute HCl extraction method for the identification of metal contamination in Antarctic marine sediments. Chemosphere 57, 491, 2004.
  • 11. RABAJCZYK A. The use of ultrasounds as well as microwave to speciation analysis Cd, Zn and Pb in precipitates bottom. Ecol. Chem and Eng. S1, 13, 167, 2006 [In Polish].
  • 12. NAMIEŚNIK J., ŁUKASIAK J., JAMRÓGIEWICZ Z., TORRES L. Preparation of environmental samples for analysis. WNT, Warszawa, 2000 [In Polish].
  • 13. NAKASHIMA S., STURGEON R.E., WILLIE S.N., BERMAN S.S. Acid digestion of Marine samples for trace element analysis using microwave heating. Analyst 113, 159, 1988.
  • 14. BETTINELLI M., BARONI U., PASTORELLI N. Microwave oven sample dissolution for the analysis of environmental and biological materials. Anal. Chim. Acta 225, 159, 1989.
  • 15. DAVIDSON Ch.M., THOMAS R.P., MCVEY S.E., PERALA R., LITTLEJOHN D., URE A.M. Evaluation of a sequential extraction procedure for the speciation of heavy metals in sediments. Anal. Chim. Acta 291, 277, 1994.
  • 16. TESSIER A., CAMPBELL P. G.C., BISSON M. Sequential extraction procedure for the speciation of particulate trace metals. Anal. Chem. 51, 844, 1979.
  • 17. LOSKA K., WIECHUŁA D., CEBULA J. Changes in the forms of metals occurrence in bottom sediments under conditions of artificial hypolimnetic aeration of Rybnik reservoir. Southern Poland. Pol. J. Environ. Stud. 9(6), 523, 2000.
  • 18. WIECHUŁA D., KWAPULIŃSKI J., LOSKA K. Speciation on the investigation of zinc biovailability in bottom sediments the “Dziećkowice” reservoir. Scientific Papers “Human and Environment” PAN, 33, 183, 2002 [In Polish].
  • 19. VICENTE-BECKETT V.A. Trace metal levels and speciation in sediments of same Philippine natural waters. Sci. Total Environ. 125, 345, 1992.
  • 20. ZERBE J., SOBCZYŃSKI T., ELBANOWSKA H., SIEPAK J. Speciation of heavy metals in bottom sediments of lakes. Pol. J. Environ. Stud. 8(5), 331, 1999.
  • 21. DOJLIDO J.R. Chemistry of surface water. Wydawnictwo Ekonomia i Środowisko, Białystok, 1995 [In Polish].

Typ dokumentu

Bibliografia

Identyfikatory

Identyfikator YADDA

bwmeta1.element.agro-article-901ae8ab-245f-44fa-b749-7ff2b916339c
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